Development of a harmonised method for the profiling of amphetamines: I. Synthesis of standards and compilation of analytical data

Aalberg, Laura and Andersson, Kjell and Bertler, Christina and Borén, Hans and Cole, Michael D. and Dahlén, Johan and Finnon, Yvonne and Huizer, Henk and Jalava, Kaisa and Kaa, Elisabet and Lock, Eric and Lopes, Alvaro and Poortman-van der Meer, Anneke and Sippola, Erkki (2005) Development of a harmonised method for the profiling of amphetamines: I. Synthesis of standards and compilation of analytical data. Forensic Science International, 149 (2-3). pp. 219-229. ISSN 1872-6283

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Abstract

Reference material was synthesised for 21 substances that are frequently present as synthetic impurities, i.e. by-products, in illicitly produced amphetamine. Each of these substances is a typical by-product for at least one of the three approaches most often used to synthesise amphetamine, namely, the Leuckart, the reductive amination of benzyl methyl ketone, and the nitrostyrene routes. A large body of data on the substances was recorded, including the following: mass spectra, ultraviolet spectra, Fourier transform infrared spectra, infrared spectra in gas phase, and 1H NMR and 13C NMR spectra.

Item Type:	Journal Article
Keywords:	Amphetamine, Profiling, Impurities, Synthesis, Infrared spectroscopy, Gas chromatography–mass spectrometry, 1H NMR, 13C NMR, UV
Faculty:	ARCHIVED Faculty of Science & Technology (until September 2018)
Depositing User:	Repository Admin
Date Deposited:	05 May 2010 15:37
Last Modified:	08 Jun 2020 11:55
URI:	http://arro.anglia.ac.uk/id/eprint/97987

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